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Kinetic Capillary Electrophoresis(KCE): A conceptual Platform for Kinetic Homogeneous Affinity Methods
by Sergey N. Krylov Details Kinetic Capillary Electrophoresis is a family of methods for studying binding of biopolymers, measuring rate constants, binding constants, and in some cases providing mechanistic details. This annimation illustrates several kinetic CE modes and their effect on the complex formation and dissociation. Rating: 0.0/5 (0 votes cast) |
Tunable Monochromator Movie
by Thomas G. ChasteenChasteen Details This Quick Time movie illustrates and describes to operation of a Czerny-Turner monochromator. The slits, mirrors, grating and grating scan are described in the production of a specific wavelength at the outlet slit. The movie is a companion to the double beam spectrometer animation. Rating: 1.7/5 (3 votes cast) |
Affinity Chromatography
by Sapna Deo Details Using exposition, graphics, and commercial videos, this module teaches the theory and application of affinity chromatography in the characterization of proteins, nucleic acids, and other biochemical/biomedical systems. Problems and application examples support the tutorial material. Rating: 0.0/5 (0 votes cast) |
Animations and Simulations in the Teaching of Analytical Sciences
by Cynthia Larive Details This article by Cynthia Larive, published in the "ABCs of Teaching Analytical Science" series of the journal Analytical and Bioanalytical Chemistry, will be of interest to faculty members teaching courses in the analytical sciences. The article provides a good introduction to the animations, simulations, and other on-line resources available on the internet. More important, it encourages instructors to develop a teaching philosophy that emphasizes the use of these materials. Rating: 0.0/5 (0 votes cast) |
Biological Animation Library
by Dolan DNA Learning Center, Cold Springs Harbor Lab Details This site produced by the Dolan DNA Learning Center of the Cold Springs Harbor Laboratory contains a number of high quality animations that explain processes important in bioanalytical chemistry. For example, one animation illustrates the process of Sanger sequencing and another explains what Gene Chips are and how they work. PCR, gel electrophoresis, cloning, model organisms and stem cell lines are also treated. The site allows the animations to be viewed or downloaded for PC or Mac, which means that they can be easily incorporated into lectures. Rating: 0.0/5 (0 votes cast) |
ELISA Animated Virtual Laboratory
by Howard Hughes Medical Institute Details This animated virtual laboratory, produced by HHMI, addresses concepts related to analytical immunoassay including the basis of humoral immunity,the foundation of ELISA, potential errors in conducting an ELISA and the sensitivity and specificity of diagnostic tests. This site has several layers including a laboratory notebook that provide experimental protocols for each step. This animation requires Shockwave to view, which is available as a free download. Rating: 4.0/5 (1 vote cast) |
Fundamentals of GC/MS
by Shimadzu Europa GmbH Details This tutorial provides an excellent introduction into the fundamentals of GC/MS. The tutorial consists of five sections: An introduction of mass and types of ions, ionization modes, hardware, figures of merit describing mass analyzer performance, and qualitative methods of GC/MS analysis - including library searches. Each section contains animations or simulations of chemical and physical interactions that pertain to mass spectrometry such as gas-phase ionization processes, fragmentation, mass analyzers, the importance of a vacuum, and detectors. A basic introduction to gas-liquid chromatography is also provided. The tutorial is intended to describe GC/MS at an introductory level, but does include theory at an intermediate level, which may be included or not depending on the intended audience. Information is presented in a Powerpoint style, and each figure has a Details tab which provides additional information on the subject. This website has excellent pedagogical value for students and new practitioners. Rating: 3.0/5 (1 vote cast) |
X-ray Diffraction
by Peter Goodhew Details This site is a good freshman or sophomore level introduction to diffraction and its application to studying crystal structure. Because it's very visual and interactive, it engages the student. It's not mathematical enough for an upper level course. The basics of diffraction are covered with excellent interactive demos. Demos are great as a supplement but not as a stand alone module on diffraction. Rating: 0.0/5 (0 votes cast) |
Animated Vibrational Modes of Triatomic Molecules
by American Chemical Society Details Molecular vibration modes are discussed using animation to depict atomic motion. As examples, the fundamental vibrational modes and their composite superposition are demonstrated for sulfur dioxide and carbon dioxide. A brief overview of the approach for calculating molecular vibrational modes is included with references to basic literature on the topic. Atomic motion resulting from the superposition of fundamental modes is discussed in relation to effects of molecular vibrations on reactivity. The site is a Journal of Chemical Education Online article. QuickTime is required to view the animations. Rating: 0.0/5 (0 votes cast) |
The Geometer's Sketchpad - Least Squares
by Java Sketchpad Details This site provides a java-based demonstration of how a least-squares analysis works. The applet opens with a set of data points with a superimposed line. By clicking and dragging, the user can move the data points and change the slope and/or the y-intercept of the line. The residual error for each data point is shown as a square whose area increases the greater the vertical distance between the point and the line. A total sum-of-squares also is shown. By adjusting the slope and y-intercept, the user can try to find the optimum line by minimizing the total sum-of-squares. By moving data points, users also can explore the effect of outliers. The site does not provide an explanation of the mathematical details of a least-squares analysis, nor does it explain the significance of the sum-of-squares. Nevertheless, instructors will find that this is a useful tool for illustrating a least-squares analysis. Rating: 4.5/5 (2 votes cast) |
SIMS Animation
by Barbara Garrison Details You can watch simulations of atoms and molecules colliding with a metallic matrix. See crystal structures disrupted and atoms sputtered. Rating: 0.0/5 (0 votes cast) |
ICP-MS
by Jenna Worley and Steve Kvech Details This site provides the principles of ICP-MS from sample introduction, ionization to MS quadrapole analysis. Excellent illustrative schematics of the main process in ICP-MS and pictorials of component parts. This has photos of the detector horn; photos of the actual quadrapoles; and of the plasma which are nice. The site has animations showing the nebulization (although not really related to any physical operation) and to the quadrapole. This material would serve as an excellent reference resource by students at the upper undergraduate and beginning graduate level. The detection levels for 27 elements are listed in a table. Rating: 0.0/5 (0 votes cast) |
Chemical Separations
by James K. Hardy Details This site contains complete notes in a PowerPoint-like presentation for a chemical separations course. It covers a wide variety of topics, including distillation, extraction, gas chromatography, liquid chromatograpy, chromatography theory, instrumentation, electrophoresis, field flow fractionation, and affinity chromatography. It covers these topics thoroughly using a clear, consistent, and simple presentation style. Links to major topics like GC, LC, and electrophoresis provide specific information about the theory, instrumentation, and practice related to these techniques. The site also contains many annimations illustrating important separation processes. Rating: 3.0/5 (1 vote cast) |
Rice virtual lab in statistics
by David Lane Details This site is devoted to statistical tests and demonstrations of their use and was created with the support of the National Science Foundation. One section is a complete reference guide - the online statistics textbook, with detailed descriptions of all things statistical. The second, and most fun section, is simulations/demonstrations section where nearly twenty statistical tests are demonstrated with interactive Applets. Each Applet has clear instructions for use with details on the test demonstrated. A third section gives case studies where statistics have played a role, illustrating theory with specific analyses from court cases to who is buying iMacs. Rating: 0.0/5 (0 votes cast) |
Animation of diode array detection in HPLC
by TRSL Details This animation site deals specifically with diode array detection for liquid chromatography. The animations are short (one to two minutes) and can easily be shown in class as part of a lecture. They are extremely helpful in illustrating key components and concepts of chromatographic systems. Users are encouraged to explore the site and the other brief animations as well. Separate links to other simulations by the same company (TRSL) are also listed on ASDL. This site requires FLASH version 7 or higher in order to work properly. Rating: 0.0/5 (0 votes cast) |
Craig countercurrent extraction machine applet
by Prof. C.E. Efstathiou Details This site provides a useful applet that demonstrates countercurrent extraction. The explanation of the method is short, but good. The level is appropriate for undergraduate students. The Applet itself is well designed and provides a useful exercise for students around which homework or small-group waork could be developed. The use of color is particularly helpful. The same author has a larger collection of applets about instrumentation and other analytical concepts in the ASDL collection. It can be found by searching the ASDL library using 'applets' as the keyword, or going to the site: http://www.chem.uoa.gr/applets/Applet_Index2.htm Rating: 0.0/5 (0 votes cast) |
Applets for Chromatography, Signal Processing and General Analytical Chemistry
by Prof. C. E. Efstathiou Details This site offers Java-based applets as organized in 4 categories: analytical and general chemistry, instrumental chemical analysis, instrumentation/signal processing, data analysis/chemometrics. Each applet includes a short introduction followed by a user controlled input of experimental conditions, such as seen for diffusion in electrochemistry. Rating: 5.0/5 (1 vote cast) |
Animated Webpage Explaining STM
by Michael Schmid Details This is an animated gif that illustrates how scanning tunneling microscopy (STM) works. As such it is valuable to students and faculty interested in learning about this important surface analysis technique. Rating: 0.0/5 (0 votes cast) |
Overview of Scanning Probe Microscopy Techniques
by nanoScience Instruments Details This manufacturer's site offers a brief, readable, and well-illustrated introduction to several important methods in scanning probe microscopy (SPM), including STM, AFM, and NSOM. "Education links" include 3-d animations from surface scans utilizing these techniques. An excellent "Suggested Reading" section contains links to on-line texts and references to books covering SPM and other topics in nanoscience. Rating: 0.0/5 (0 votes cast) |
Principles of Scanning Probe Microscopy
by Joost Frenken Details This site offers a beautifully illustrated introduction to the principles of scanning probe microscopy. The text is interspersed with links to additional information, much of it from the Interface Physics Group at Leiden University. There are several included animations and links to picture galleries which illustrate both principles and utilization of scanning probe microscopy. An additional "links" page takes the user to sites of research groups involved in ongoing developmental work in surface science. Rating: 0.0/5 (0 votes cast) |
HPLC, LC-MS, and FTIR sites
by Shula Levin Details This site contains a considerable amount of information on HPLC, LC-MS, and FTIR via linked sites by the same author and some vendor sites. It may require considerbale time to follow the links to find specific information, but as a collection of sites related to HPLC and FTIR it is quite useful as a teaching resource. There are some interesting animations that might be helpful for students to understand how these instruments work. Rating: 0.0/5 (0 votes cast) |
Chemistry-Based QuickTime Movies, Animations, and Streaming Audio
by Chasteen, Thomas G. Details Downloadable animations and movies for analytical instruments and processes. Formats in QuickTime, GIF animations, and Flash animations. Rating: 0.0/5 (0 votes cast) |
Origin of Chromatography
by Lisensky, George Details This site has a series of links to QuickTime movies that animate the chromatographic process. The movies show the effect of changing K, L, and N on peak width and separation. The site is useful in combination with other sources that explain the background theory. Rating: 0.0/5 (0 votes cast) |
GC/MS with animations
by Dr. Thomas G. Chasteen Details This site contains a good review of GC detectors that is linked to animated files describing the hardware and principles of operation for GC/MS. From this site, one can also get to multiple other animations about a variety of analytical topics. Rating: 0.0/5 (0 votes cast) |
Kinetic Capillary Electrophoresis(KCE): A conceptual Platform for Kinetic Homogeneous Affinity Methods
by Sergey Krylov Details Kinetic Capillary Electrophoresis is a family of methods for studying binding of biopolymers, measuring rate constants, binding constants, and in some cases providing mechanistic details. This Online Article is a presentation by the originators of this family of techniques ready for classroom or independent use. Rating: 0.0/5 (0 votes cast) |
Capillary electrophoresis movie
by Thomas Chasteen Details This website is an animation describing aspects of CE separations, including electroosmotic flow, the separation, injection (hydrodynamic and electrophoretic) and detection (direct and indirect). Rating: 0.0/5 (0 votes cast) |
Separation Science Animations
by TRSL Details This site from TRSL is the main site that links to many animations related to how chromatography systems work. Most of the animations are quite good and would be helpful to students when trying to visualize what occurs in an instrument during an separation (e.g. injection, detection, etc.). Rating: 0.0/5 (0 votes cast) |
Landmark Instruments of Chemistry
by Richard H. Bromund Details This website effectively uses animated movies combined with text explanations to describe the processes in FT-IR interferometry, TLC, GC and magnetic sector mass spec. It is effective in illustrating processes that are otherwise difficult to visualize. These materials are excellent visualization tools that can be incorporated into lectures readily. Rating: 4.0/5 (1 vote cast) |
Animation of sample loop HPLC injections
by TRSL Details This site deals specifically with sample loop injections in liquid chromatography. The animations are short (one to two minutes) and can easily be shown in class as part of a lecture. They are extremely helpful in illustrating key components and concepts of chromatographic systems. Users are encouraged to explore the site and the other brief animations as well. Separate links to other simulations by the same company (TRSL) are listed below. Rating: 0.0/5 (0 votes cast) |
Animation of Dual Head HPLC Pump
by TRSL Details This animation site deals specifically with dual head LC pumping. The animations are short (one to two minutes) and can easily be shown in class as part of a lecture. They are extremely helpful in illustrating key components and concepts of chromatographic systems. Users are encouraged to explore the site and the other brief animations as well. Separate links to other simulations by the same company (TRSL) are also listed on ASDL. Rating: 0.0/5 (0 votes cast) |
Animation of Quadrupole GC-MS detection
by TRSL Details An animation site which deals specifically with quadrupole mass spectrometry detection for chromatography. The animations are short (one to two minutes) and can easily be shown in class as part of a lecture. They are extremely helpful in illustrating key components and concepts of chromatographic systems. Users are encouraged to explore the site and the other brief animations as well. Separate links to other simulations by the same company (TRSL) are also listed on ASDL. Rating: 0.0/5 (0 votes cast) |
Animation of GC solvent focusing
by TRSL Details This site has very good animations related to separations. It deals specifically with solvent focusing in gas chromatography. The animations are short (one to two minutes) and can easily be shown in class as part of a lecture. They are extremely helpful in illustrating key components and concepts of chromatographic systems. Users are encouraged to explore the site and the other brief animations as well. Separate links to other simulations by the same company (TRSL) are also listed on ASDL. Rating: 0.0/5 (0 votes cast) |
Analytical Instruments and Spectroscopic Concepts
by Chasteen, Thomas G. Details Primers for different analytical techniques (HTML, PDF). Also links to animations and audio descriptions of analytically related concepts. Techniques include atomic absorption, spectrophotometry, chemiluminescence, gas chromatography, mass spectrometry, and atomic emission. Rating: 1.0/5 (1 vote cast) |
Cyclic Voltammetry Simulator
by Vining, William Details This simulator allows the modeling of responses from experiments in cyclic voltammetry, and is applicable to a wide variety of parameters. Excellent instructional aids in text form include description of electrochemical reversibility, diffusion, instrumentation and interpretation of cyclic voltammograms, with real-time demonstration of parameter changes. Rating: 4.5/5 (2 votes cast) |
NMR animation
by Françoise Sauriol Details This site has very nicely animated tutorials on NMR with sufficient depth to be useful to the non NMR savy. The animations are accompanied by short descriptions so that the processes displayed can be understood by the viewer. This site goes beyond just showing precession. There are nice animations showing the effect of different pulses, including composite pulses on the magnetization, the effects of magnetic gradient pulses to measure diffusion and do coherence pathway selection. Other aspects are less useful since they basically just present material that could be found in a book in an animated format. The site is useful for teaching in a lecture setting. Students will find the images appealing. Rating: 0.0/5 (0 votes cast) |
FTIR Spectrometry
by Paul L. Edmiston Details The site demonstrates principles behind the operation of the interferometer in an FTIR spectrometer. Graphics and interactive movies are used. Examples start from a single wavelength and build to the superposition of multiple wavelengths. The connection between an interferogram and a frequency domain spectrum is discussed. Rating: 0.0/5 (0 votes cast) |
Scanning Electrochemical Microscopy
by Dr. David O. Wipf Details A concise synopsis of scanning electrochemical microscopy (SECM) with an extensive bibliography. Excellent color graphics and short animations are used effectively to demonstrate the instrumental essentials, physical aspects, and operational modes of SECM. Rating: 0.0/5 (0 votes cast) |
Chromatography
by Dan Damelin Details An introductory site about chromatography that does not go into great depth. However, the simulation of paper chromatography is worth exploring with students as it illustrates that the separation of compounds relies on the difference in the solutes affinities for the mobile phase relative to the stationary phase. Because of its apparent simplicity, this simulation has significant pedagogical potential and could be used in a variety of ways in class to explore the factors governing chromatographic separations. Rating: 0.0/5 (0 votes cast) |
Instrumentation on the web
by Thomas G. Chasteen Details The teaching of instrumentation is discussed using animationsm, many of which were produced by the authors. Site contains numerous links and many instrumentation animations. Rating: 0.0/5 (0 votes cast) |
Animations in an Instrumental Methods Chemistry Class?
by Thomas G. Chasteen Details This website provides an introduction to animations as a tool for teaching instrumental techniques in the instrumental analysis course - why one might wish to use animations, some information on how to go about developing them, and it provides a number of examples of animations for analytical instrumentation. One problem with the site is that some of the animations emphasize instrumentation that is not frequently used today. For example, the section on ICP shows an instrument with the classical Rowland Circle configuration and the section on GC-MS shows an animation of a sector mass spectrometer. Nonetheless, the site should prove a valuable resource to college educators teaching analytical chemistry. Rating: 0.0/5 (0 votes cast) |
Animation of single wavelength UV-vis detection for HPLC
by TRSL Details This site deals specifically with single wavelength UV-vis detection for liquid chromatography. The animations are short (one to two minutes) and can easily be shown in class as part of a lecture. They are extremely helpful in illustrating key components and concepts of chromatographic systems. Users are encouraged to explore the site and the other brief animations as well. Separate links to other simulations by the same company (TRSL) are also listed on ASDL. Rating: 0.0/5 (0 votes cast) |
GC coating animation
by TRSL Details This site is one in a series of sites with very good animations related to separations. This animation deals specifically with solute retention in GC. The animations are short (one to two minutes) and can easily be shown in class as part of a lecture. They are extremely helpful in illustrating key components and concepts of chromatographic systems. Users are encouraged to explore the site and the other brief animations as well. Separate links to other simulations by the same company (TRSL) are also listed on ASDL. Rating: 0.0/5 (0 votes cast) |
Animation of GC flame ionization detector
by TRSL Details This site is one in a series of sites with very good animations related to separations. This animation deals specifically with flame ionization detection in GC. The animations are short (one to two minutes) and can easily be shown in class as part of a lecture. They are extremely helpful in illustrating key components and concepts of chromatographic systems. Users are encouraged to explore the site and the other brief animations as well. Separate links to other simulations by the same company (TRSL) are also listed on ASDL. Rating: 0.0/5 (0 votes cast) |
Fluorescence Detection Animation
by TRSL Details This animation site deals specifically with fluorescence detection for liquid chromatography. The animations are short (one to two minutes) and can easily be shown in class as part of a lecture. They are extremely helpful in illustrating key components and concepts of chromatographic systems. Users are encouraged to explore the site and the other brief animations as well. Separate links to other simulations by the same company (TRSL) are also listed on ASDL. Rating: 0.0/5 (0 votes cast) |
Animation of Single Head Check Valve HPLC Pump
by TRSL Details This animation site is specifically about reciprocating pumps for liquid chromatography. The animations are short (one to two minutes) and can easily be shown in class as part of a lecture. They are extremely helpful in illustrating key components and concepts of chromatographic systems. Users are encouraged to explore the site and the other brief animations as well. Separate links to other simulations by the same company (TRSL) are also listed on ASDL. Rating: 0.0/5 (0 votes cast) |
GC Electron Capture Detector Animation
by TRSL Details This site is one in a series of sites with very good animations related to separations. This animation deals specifically with electron capture detectors. The animations are short (one to two minutes) and can easily be shown in class as part of a lecture. They are extremely helpful in illustrating key components and concepts of chromatographic systems. Users are encouraged to explore the site and the other brief animations as well. Separate links to other simulations by the same company (TRSL) are also listed on ASDL. Rating: 0.0/5 (0 votes cast) |
Split Injection GC
by TRSL Details This animation site deals specifically with split injection in gas chromatography. The animations are short (one to two minutes) and can easily be shown in class as part of a lecture. They are extremely helpful in illustrating key components and concepts of chromatographic systems. Users are encouraged to explore the site and the other brief animations as well. Separate links to other simulations by the same company (TRSL) are also listed on ASDL. Rating: 0.0/5 (0 votes cast) |
Animation of pulse dampner in HPLC
by TRSL Details This animation site deals specifically with pulse dampners is LC and could help in a general lecture about LC pumps. The animations are short (one to two minutes) and can easily be shown in class as part of a lecture. They are extremely helpful in illustrating key components and concepts of chromatographic systems. Users are encouraged to explore the site and the other brief animations as well. Separate links to other simulations by the same company (TRSL) are also listed on ASDL. Rating: 0.0/5 (0 votes cast) |
GC Splitless Injection Animation
by TRSL Details This site is one in a series of sites with very good animations related to separations. This animation deals specifically with splitless injection in GC. The animations are short (one to two minutes) and can easily be shown in class as part of a lecture. They are extremely helpful in illustrating key components and concepts of chromatographic systems. Users are encouraged to explore the site and the other brief animations as well. Separate links to other simulations by the same company (TRSL) are also listed on ASDL. Rating: 0.0/5 (0 votes cast) |
Atomic Absorption Instruction Module
by University of Michigan Dearborn Science Learning C Details An introduction to Atomic Absorption Spectroscopy for the non-chemist or new user. Rating: 5.0/5 (1 vote cast) |
Titration of an Unknown Acid or Base
by Blauch, David N. Details This website contains a JAVA applet that simulates the titration of an unknown acid or base, and provides a graphical output of the titration curve. The unknown compounds are taken from a list of amino acids. Students set up the parameters of the titration, and then create a simulated pH curve. From this they are able to identify the unknown compound from the list, and determine the acid dissociation constant(s) from the titration data. Rating: 0.0/5 (0 votes cast) |
Chemistry Experiment Simulation, Tutorials and Computer Animations for College Chemistry
by Tom Greenebowe Details After instructions on what computer programs will be needed, you can simulate chemical processes related to electrochemistry, acid-base chemistry & stoichiometry. Rating: 0.0/5 (0 votes cast) |
Electromagnetic waves and circular dichroism:an animated tutorial
by Szilagyi, Andras Details This website provides a tutorial on electromagnetic waves using animated graphics. The tutorial gives the student the ability to visualize, plane, and circularly polarized waves, the superposition of various types of polarized waves, and the change that results when the EM waves interact with matter. Rating: 0.0/5 (0 votes cast) |
Introduction to Chemical Equilibria
by Blauch, David N. Details An interactive set of applet-based demonstrations (many modeled as experimental measurements) that illustrate the concepts and calculations of chemical equilibria. The site demonstrates equilibrium processes in a reaction vessel by plotting the concentration of reactants and products over time. The site would be a good supplement for a class in general chemistry or quantitative analysis. Rating: 0.0/5 (0 votes cast) |
Analytical Chemistry
by Hardy, James K. Details Lecture notes for 1st semester are on titrations, gravimetry, kinetics and electrochemistry (redox). Potentiometry, coulometry, voltammetry, spectroscopic and separation methods are presented during 2nd semester, illustrated with QuickTime animations. Rating: 0.0/5 (0 votes cast) |
Basics of NMR
by Hornak, Joseph P. Details An online text on the basics of Nuclear Magnetic Resonance (NMR) spectroscopy. The text contains information especially appropriate for the novice, but topics are treated at sufficient depth to be useful for more advanced students. This resource features animations that illustrate complex NMR concepts such as precession and the rotating frame of reference. Rating: 0.0/5 (0 votes cast) |
* editor's choice Analytical Chemistry 2.0
by David Harvey Details A complete textbook for Quantitative Analysis is freely downloadable. Teach yourself Analytical Chemistry, or be part of a class on the subject. Rating: 5.0/5 (2 votes cast) |
Introduction to Lasers
by Carol Korzeniewski Details Lasers are preferred light sources for high resolution or time-resolved optical spectroscopy. This module introduces the workings of lasers and gives examples of common designs. Rating: 0.0/5 (0 votes cast) |
Electro-Optics Handbook
by Burle Details The Electro-Optics handbook is a 14 chapter reference text which addresses sources of radiation, including lasers, detection and detectors, photometric quantities, and geometric optics. Specific details can be found with the extensive appendix. The text is technical and lists equations without derivations. Rating: 0.0/5 (0 votes cast) |
Affinity Chromatography
by Sapna Deo Details Using exposition, graphics, and commercial videos, this module teaches the theory and application of affinity chromatography in the characterization of proteins, nucleic acids, and other biochemical/biomedical systems. Problems and application examples support the tutorial material. Rating: 0.0/5 (0 votes cast) |
Analytical Electrochemistry: Basic concepts
by Richard S. Kelly Details This module focuses on the basic concepts involved in dynamic electrochemistry when the net current is not zero - the combination of mass transfer and electrochemical reactions at the interface between solids and fluids. It is at an introductory level appropriate for undergraduates in their sophomore or junior years. Rating: 3.3/5 (4 votes cast) |
Atomic Emission Spectroscopy
by Alexander Scheeline Details A learning module that explains the instrumental systems and interactions involved in atomic emission for elemental analysis. Completion of the module will leave the learner with knowledge of optics, plasma sources, and trade-offs in choosing the right instrument for a given analytical task. Rating: 0.0/5 (0 votes cast) |
Analytical Electrochemistry: Potentiometry
by Erin Gross Details This courseware module is structured for either a lecture presentation or self-study tutorial on analytical potentiometry. The level of presentation spans upper high school to college students. Topics include historical background, theory/principles, instrumentation, pH electrodes, experimental examples, and troubleshooting tips. Rating: 4.0/5 (1 vote cast) |
Fluorine NMR
by J. T. Gerig Details This article describes the use of fluorine (19F) NMR for the analysis and structure determination of biomaterials. Using a traditional text-with-figures format, the article gives an overview of the synthesis of 19F spin-labeled materials and detailed descriptions of 19F chemical shifts and relaxation phenomena as applied to both primary and tertiary structure determinations of biochemical interest. Rating: 2.0/5 (1 vote cast) |
Fluorescence Correlation Spectroscopy
by Petra Schwille and Elke Haustein Details Previously published as part of an online biophysics textbook, the article has rich and fairly complete scientific content. Rating: 0.0/5 (0 votes cast) |
A Pictorial Representation of Product Operator Formalism: Non-Classical Vector Diagrams for Multidimensional NMR
by Biophysical Society; Donne and Gorenstein Details This site presents a pictorial description of the product operator formalism using a non-classical vector approach. This approach allows for the representation of any arbitrary multidimensional or heteronuclear NMR experiment. A description of a complete set of 16 vector representations for weakly-coupled two-spin (I=1/2) systems is given followed by an extension of this set to three-spin systems. Finally the concepts of coherence transfer, multiple quantum spectroscopy and phase cycling are illustrated using 2D COSY, 2D INADEQUATE, DEPT and sensitivity-enhanced HSQC as examples. The content is geared to those that have some background in NMR spectroscopy, and is probably most appropriate for a graduate course in NMR. This site can be used as a teaching tool as well as by practitioners who would like to easily deconstruct a pulse sequence for a better understanding of the “spin engineering” involved. Rating: 0.0/5 (0 votes cast) |
Fundamentals of NMR
by Biophysical Society, Thomas James Details This e-text presents an introduction to the fundamentals of NMR covering magnetic resonance, pulsed NMR, relaxation, chemical shift, spin-spin coupling, the nuclear Overhauser effect and chemical exchange. Rating: 0.0/5 (0 votes cast) |
Introduction to X-ray Diffraction (XRD)
by Heather Bullen Details This learning module presents the fundamentals of X-ray Diffraction for characterizing molecular structure in a form useful both as lecture notes and for self-study. Rating: 0.0/5 (0 votes cast) |
Introduction to Data Analysis
by David Harvey Details Means, standard deviation, and deciding if two results are different at some level of statistical significance is the basis for analytical decision making. This module teaches students how to use t-tests, Q-tests, and to tell when differences are statistically real. Rating: 5.0/5 (1 vote cast) |
Green Chemistry (2nd edition)
by Stanley Manahan Details Measurement science used to characterize environmentally important species is a central aspect of this textbook and accompanying lecture support/PowerPoint presentations. In addition to discussing the hows and whys of measurement, the discussion of measurements up to 2007 as related to the future of the environment provides a context for learning the material. Rating: 0.0/5 (0 votes cast) |
Atomic Structure and the Periodic Chart
by Stephan Lower. Simon Fraser University Details Online eText gives a thorough descriptive overview of atomic structure. The site is organized into sections on light particles and waves, the Bohr atom, the quantum atom, atomic electron configuration, and periodic properties. Hyperlinks to interactive demonstrations of physiochemical principals with questions posed are included. At the end of each section, flowcharts, called "concept maps" guide the students from basic principles to working concepts. Rating: 0.0/5 (0 votes cast) |
Introduction to Scanning Probe Microscopy
by Heather Bullen Details This learning module teaches the principles behind scanning tunneling microscopy and atomic force microscopy. The module includes example applications and ample literature citations. Rating: 0.0/5 (0 votes cast) |
NIST Engineering Statistics Handbook
by NIST Details This site provides a comprehensive electronic handbook on statistics for scientists and engineers. Topics include graphical approaches for exploratory data analysis, the characterization of measurement processes, the construction of statistical models for predicting and/or optimizing process, experimental design, process control monitoring, significance testing and the evaluation of product reliability. Although the site may be too detailed and complex for an undergraduate student to navigate without significant guidance, it is a useful resource for graduate students and practicing analytical chemists. Individual chapters can be downloaded as pdf files. The handbook provides numerous case studies and examples. Rating: 4.0/5 (1 vote cast) |
ICP-MS
by Jenna Worley and Steve Kvech Details This site provides the principles of ICP-MS from sample introduction, ionization to MS quadrapole analysis. Excellent illustrative schematics of the main process in ICP-MS and pictorials of component parts. This has photos of the detector horn; photos of the actual quadrapoles; and of the plasma which are nice. The site has animations showing the nebulization (although not really related to any physical operation) and to the quadrapole. This material would serve as an excellent reference resource by students at the upper undergraduate and beginning graduate level. The detection levels for 27 elements are listed in a table. Rating: 0.0/5 (0 votes cast) |
Reliable Measurements: A Guidebook for Trace Analysts
by Dr. Paul Gaines Details Provides a comprehensive resource on sample preparation and analysis for those interested in elemental determinations by atomic spectrometry, especially ICP-OES and ICP-MS. Issue such as sources of contamination, detection limits, sample preparation, standard stability, and method validation are well covered. Rating: 0.0/5 (0 votes cast) |
Chromatography Theory
by Rochester Institute of Technology Details This site contains standard definitions related to chromatgraphy similar to treatments found in analytical textbooks. It introduces the beginning student to LC concepts relevant to biochemistry and includes a good example of choosing a mobile phase pH for a protein separation based on ion exchange. Rating: 0.0/5 (0 votes cast) |
Introduction to Capillary Electrophoresis
by Beckman Coulter Details A comprehensive overview of capillary electrophoresis and its closesly related variants. This pdf document details both theoretical and practical aspects of CE, and includes an application index and thorough bibliography. This material is appropriate for beginners or new practitioners of CE, and would be an excellent resource for instruction in instrumental techniques. Rating: 0.0/5 (0 votes cast) |
Chromatography
by Tissue, Brian M. Details Multiple links in a broad discussion of several facets of chromatography - including theoretical and instrumental aspects. Five modes of chromatography are highlighted: GC, HPLC, LC, SEC and TLC. Rating: 0.0/5 (0 votes cast) |
Basic Liquid Chromatography
by Kazakevich,Yuri Details A complete textbook of liquid chromatography by Yuri Kazakevich and Harold McNair on the Web. Extraordinarily comprehensive in its coverage of fundamental chromatographic theory and instrumentation for a website. Rating: 0.0/5 (0 votes cast) |
Introduction to Mass Spectrometry
by Siuzdak, Gary Details This site contains an on-line text on mass spectrometry at the intermediate level. The text gives good general coverage of mass spectrometry instrumentation and applications in very readable format. It contains nice diagrams that provide a visualization of the ionization and mass selection processes. It also contains an overview of applications of mass spectrometry near the end that is different than most sites related to MS. It is especially appropriate for intermediate students. Rating: 0.0/5 (0 votes cast) |
ICP Operations: A Guide for New ICP Users
by Dr. Paul Gaines Details A handbook for ICP analysis. Topics such as matrix compatibility, quality control, spectral interferences, instrument operation (e.g. sample introduction, nebulization, etc.) make this an excellent practical yet concise manual on ICP operation. Rating: 0.0/5 (0 votes cast) |
Understanding NMR
by james keeler Details This site provides links to a series of pdf files that represent chapters of an e-text on the basics of NMR. While many textbooks on NMR are available the chief merit of this one is that it has a nice chapter on the NMR instrument (ch. 5) which should be accessible to undergraduates. The text also provides a relatively mathematics-free or maybe more accurately Dirac bracket notation-free introduction to 1-D and 2-D (COSY and NOESY) experiments that would be appreciated by advanced undergraduates or beginning graduate students involved in undergraduate research experiences using NMR Rating: 0.0/5 (0 votes cast) |
Immunoassay, biosensors and other non-chromatographic methods for agrochemical analysis
by G. Shan, C. Lipton, S. J. Gee and B. D. Hammock Details This site is a comprehensive 58 page book chapter in pdf format on nonchromatographic methods of analysis for agrochemical contaminants (residues). The process of preparing and testing immunoassay tests is also discussed. Both biological and physical-based methods are discussed. In the former, it presents a wide variety of methods including the use of PCR. In the latter, it includes spectroscopy and voltammetry. Rating: 0.0/5 (0 votes cast) |
Nuclear Magnetic Resonance Spectroscopy
by William Reusch, Michigan State University Details This website serves as a primer for understanding the fundamentals of NMR spectroscopy. Plenty of useful figures and animations that enhance the understanding of nuclear spin, shielding, and how these phenomena serve as the basis for NMR. Rating: 0.0/5 (0 votes cast) |
SPR : Surface Plasmon Resonance Tutorial
by Arnoud Marquart Details Provides a straightforward introduction to the fundamentals of SPR, the genesis of the plasmon and the evanescent wave, and how SPR can be used to monitor the chemical nature of species adsorbed to the surface of a metal substrate. Rating: 0.0/5 (0 votes cast) |
Chem 212 - Separations Science
by Thomas Wenzel Details Superb website providing instructional materials in support of a problem-based learning approach to Quantitative Analysis (equilibria and separations). Materials available include textbook chapters, in-class, and out-of-class problems, a peer/peer evaluation tool, and a handout in support of a final course lab project report. The majority of materials are provided in an Adobe pdf format - very helpful for adoption by interested faculties. Rating: 0.0/5 (0 votes cast) |
The Practical Application of Light
by Melles Griot Corp. Details This commercial website is a good tutorial on optical design. While users should know a few freshman physics ideas about the nature of light and imaging, the novice optical designer can start from scratch using the material provided by Melles Griot. Rating: 0.0/5 (0 votes cast) |
Adsorption and Chromatography in Bioseparations
by Hubble, John Details This material was developed for a final year undergraduate bioseparations module. There are a number of links to sites for modeling adsorption chromatography. For example, a link to an Excel spreadsheet provides a demonstration of varying N, l, and K (or alpha)affect band separation. Other links explain adsorption isotherms in the context of bioseparations. Rating: 0.0/5 (0 votes cast) |
How People Learn: Brain, Mind, Experience, and School: Expanded Edition (2000)
by Bransford, John D. Details This page, in the National Academy Press website, gives the table of content of the book in the title of this site. As one of the "openbooks" from this press, the site allows one to search the book (approximately 400 pages) as well as download the complete book or selected portions of it. The site will be most useful to an analytical scientist interested in reading about current learning theories. Rating: 0.0/5 (0 votes cast) |
The Electronic Statistics Textbook
by StatSoft Details This electronic textbook on statistics provides both extensive and in depth coverage of statistics. Although an excellent reference for analytical chemistry students and faculty, the lack of chemistry-related practice problems or exercises may not make it an appropriate substitute for a traditional text. Rating: 0.0/5 (0 votes cast) |
The Basics of MRI
by Hornak, Joseph Details This website is an on-line textbook describing the principles of magnetic resonance imaging (MRI). The treatment is often quite mathematical, but the site also reviews all of the mathematics and physics needed to understand the material. Approximately forty clinical images can also be found on the site. This site is appropriate for students needing a stand-alone introduction to MRI. Rating: 5.0/5 (1 vote cast) |
Basics of NMR
by Hornak, Joseph P. Details An online text on the basics of Nuclear Magnetic Resonance (NMR) spectroscopy. The text contains information especially appropriate for the novice, but topics are treated at sufficient depth to be useful for more advanced students. This resource features animations that illustrate complex NMR concepts such as precession and the rotating frame of reference. Rating: 0.0/5 (0 votes cast) |
An Introduction to Surface Chemistry
by Nix, Roger Details Theoretical and descriptive material for an introductory surface science course. Topics covered include structure of surfaces and detailed information on a variety of surface analytical techniques, essentially an online text. Rating: 0.0/5 (0 votes cast) |
NMR tutorial
by Dekek Bogdal, Politechnika Krakowska Details The introduction to this site provides an entry-level introductions to NMR in a text + figures format. The site also contains two example structure elucidation problems using NMR. IR and MS data complete with hints and answers. Although the molecules are pretty simple, the examples do a good job of illustrating the structure elucidation process. The site also has data for 5 more complex structure determination problems. Rating: 0.0/5 (0 votes cast) |
Introduction to Data Analysis
by David Harvey Details Means, standard deviation, and deciding if two results are different at some level of statistical significance is the basis for analytical decision making. This module teaches students how to use t-tests, Q-tests, and to tell when differences are statistically real. Rating: 5.0/5 (1 vote cast) |
Quantitative Chemical Analysis, 6e
by Harris, Daniel C. Details This is a site with material related to Dan Harris' textbook. It is not as general as some sites but the material is of high pedagogical value. Short tutorial sections are available for many topics with extensive web linkages. "Living" graphs and Excel files illustrate important material such as pH fractional composition and statistical analysis. Students can take practice quizzes on material from the text. Full Powerpoint slideshows include nearly all of the figures contained in the text. Full set of laboratory experiments are available. Some material is not available without registering as a user. Some menus are hidden beneath buttoms of windows, and are sometime difficult to utilize. Once mastered, the site works well. The most likely users of this site are teachers and students who may be using Harris' textbook, as much of the material is keyed to it, but others may also find it useful. Rating: 4.0/5 (1 vote cast) |
Statistics for Chemists
by R. Wehrens Details Excellent comprehensive resource on statistics, including information on descriptive statistics, confidence intervals, hypothesis testing, regression, ANOVA, experimental design, and multivariate statistics. Web-based exercises are interspersed throughout the text, allowing students to practice what they are learning and to obtain immediate feedback. Rating: 0.0/5 (0 votes cast) |
Statistics for Analytical Chemistry
by Scott van Bramer Details This site provides a brief reference on statistics that both analytical faculty and students will find useful. The site includes a series of problem sets and supporting MathCAD spreadsheets. Materials available on the website can be downloaded as a pdf file. Rating: 0.0/5 (0 votes cast) |
Ohio State University General Chemistry Test Bank
by Ohio State Chemistry Details A comprehensive set of test bank questions is offered to reinforce concepts in a general chemistry course. Test banks 11-14 cover topics related to analytical chemistry including electrochemistry. Rating: 0.0/5 (0 votes cast) |
Spectroscopy
Details This site describes the theory and practice of IR and NMR spectroscopy for classroom and laboratory instruction. Although it is written for a course at the University of Colorado, Boulder, this site is appropriate for anyone doing analytical measurements with infrared or NMR. Rating: 3.0/5 (1 vote cast) |
Chem 212 - Separations Science
by Thomas Wenzel Details Superb website providing instructional materials in support of a problem-based learning approach to Quantitative Analysis (equilibria and separations). Materials available include textbook chapters, in-class, and out-of-class problems, a peer/peer evaluation tool, and a handout in support of a final course lab project report. The majority of materials are provided in an Adobe pdf format - very helpful for adoption by interested faculties. Rating: 0.0/5 (0 votes cast) |
Organic Chemistry On Line
by William Reusch Details This site covers introductory material related to the analysis of small organic molecules by mass spectrometry, UV-visible, IR, and NMR spectroscopy. A concise explanation of each approach is presented with illustrations. This would be useful for those teaching organic chemistry and for others who need a review of the topic. The section on Spectroscopy Resources at the end of the site contains a list of links to additional information plus a several links to compilations of problems (and their solutions) that challenge the student to interpret NMR or IR spectra. Rating: 0.0/5 (0 votes cast) |
Chemical Equilibrium in the Gas Phase
by Gwen Sibert, Roanoke Valley Governor's School Details This website describes gas phase equilibrium chemistry and provides a tutorial on key concepts like LeChatelier's principal and includes on-line exercises in which the reader can check their understanding. Calculations of equilibrium constants expressed in terms of pressure and concentration are presented. This site will be most useful for high school and introductory university Chemistry courses in which students are developing an understanding of equilibrium chemistry. Rating: 0.0/5 (0 votes cast) |
WebSpectra - Problems in NMR and IR Spectroscopy
by Merlic, Craig A. Details This web site provides thirty beginning, twenty-nine intermediate, and sixteen advanced NMR structure analysis problems and their solutions. For every unknown a proton and a carbon spectrum are provided. Many of the more advanced problems contain COSY and DEPT spectra as well. A particularly useful feature of this site is that the user can zoom into spectral regions in all of the spectra. Rating: 0.0/5 (0 votes cast) |
Organic Structure Elucidation Workbook
by Smith, Bradley D. Details This web site contains 64 structure elucidation problems for the qualitative analysis of organic compounds. For each problem the empirical formula, molecular weight, 500 MHz proton and 125 MHz carbon NMR spectra, IR and mass spectral data are presented. The problems are categorized as easy, moderate or difficult. Students in introductory Organic Chemistry who want practice identifying unknown compounds should find this site useful. Instructors looking for exam or classroom problems for students at this level could also take advantage of the information on this site. Rating: 0.0/5 (0 votes cast) |
The Paradigm Laboratory Project
by Heppert, Joseph A. Details This project plans to develop problem-based inquiry learning laboratories that have science majors in introductory chemistry laboratories transfer an understanding of the attitudes and methods of scientific inquiry to knowledge and experiences in their disciplines of study. Rating: 5.0/5 (1 vote cast) |
Atomic Spectroscopy in a Project-Based Lab
by Dulasiri Amarasiriwardena Details An article published in the "ABCs of Teaching Analytical Science" series of the journal Analytical and Bioanalytical Chemistry describes a project-based lab in which students investigate the distribution of Pb and As (from pesticides) in a contaminated apple orchard. Students have complete control of the lab, from designing a sampling strategy to using the primary literature to develop procedures for extracting the analytes and for their subsequent analysis by ICP-AES or ICP-MS. Rating: 5.0/5 (1 vote cast) |
Experiments in Electroanalytical Chemistry
by E. Kirowa-Eisner, D. Tzur, M. Brand and Ch. Yarnit Details This website offers educators a set of eight classical electroanalytical experiments suitable for use in a quantitative analysis, instrumental analysis, or electrochemistry course. The materials should be useful for advanced undergraduates and beginning graduate students. Experiments include coulometric, conductometric, and potentiometric titrations, stripping analysis, flow injection analysis, and polarography. It is important to note that several of the experiments use mercury or mercury coated electrodes which present safety concerns. Rating: 5.0/5 (1 vote cast) |
Quantitative NMR
by Cynthia Larive Details A learning module focused on principles and practice of NMR for quantitative analysis, an application less commonly associated with the technique than is structure determination. Links to simulation packages are included. Rating: 5.0/5 (2 votes cast) |
Electrochemical Detection of Phenol Utilizing a Synthesized Sonogel-carbon Zirconium Oxide
by Suzanne Lunsford Details This experiment is designed for senior undergraduate students in an inorganic chemistry course. Students are asked to synthesize a sonogel-carbon electrode that is modified with a ZrO2 sol-gel and to compare the results to those of an unmodified electrode for the detection of phenol. Rating: 5.0/5 (1 vote cast) |
Laboratory Orientation and Testing of Body Fluids and Tissues for Forensic Analysts
by Bill Tilstone Details This web site is part of the President's DNA Initiative and is devoted to an overview of historical and contemporary techniques to characterize body tissues. The first part of the course covers basic laboratory procedures, safety requirements for laboratory personnel and emphasizes quality control and quality assurance in the laboratory. The second section deals with serological techniques for characterizing specimens such as saliva, semen, blood and urine Identification and individual utilizing polymorphic enzymes are also covered. The site is designed as an on-line short course with excellent graphic support. The user must register and secure a readily obtainable password prior to entering the site. Rating: 5.0/5 (1 vote cast) |
Analytical Electrochemistry: A Laboratory Manual
by Theodore Kuwana Details This labware module contains directions for seven experiments in analytical electrochemistry. The experiments are designed to illustrate fundamentals of electrode reactions as applied to readily accessible redox reactants. They provide insight to dynamic electrochemistry for scientists at all levels of training. Activation procedures to prepare glassy carbon electrodes are provided in a TechNote. Rating: 5.0/5 (1 vote cast) |
A Biosensor for Fullerenes and Carbon Nanotubes
by A. N. Kirschner, B. F. Erlanqer, S. R. Wilson Details This site contains an article that describes the use of surface plasmon resonance (SPR) spectroscopy to monitor real-time protein binding with fullerenes and carbon nanotubes. The introductory section provides a brief description of SPR and how it works. It next talks about the features of the Texas Instrument's SPR, known as Speetra, which is a small self-contained apparatus for light measurements. It is followed by sections discussing the properties of fullerenes and carbon nanotubes, and the methods of surface binding with monoclonal antibodies. Experimental procedures are discussed followed by example results. An analysis and explanation of results in the concluding discussion section provides useful guidance to students and practitioners. Rating: 5.0/5 (1 vote cast) |
Forensics in the classroom
by Court TV Details This site uses crime scene scenarios to introduce concepts of biology, chemistry, and physics in a way designed to excite interest in the applications of forensic investigations. Students conduct a variety of experiments including paper chromatography analysis, hair analysis, pH testing, fingerprinting, and handwriting analysis to experience forensic science technology. The site is a collaboration between the American Academy of Forensic Sciences and Court TV designed for middle and high school curriculums. Rating: 5.0/5 (1 vote cast) |
Physical Chemistry Online
by Theresa Julia Zielinski Details Physical Chemistry Online (PCOL) Is a collection of physical chemistry modules that address specific concepts in an open-ended, collaborative fashion. The PCOL collection contains fifteen guided inquiry modules covering five broad topics: thermodynamics, kinetics, polymers, computational chemistry, and spectroscopy. Many modules provide the students with an industrial context auch as the evaluation of raw materials or the development of new products. Students that participate in these modules are expected to work with their peers in a collaborative fashion and encouraged to share their results with groups at other participating institutions. The website contains an Instructor Handbook that provides the History Of PCOL, Module Development, and Ideas/resources related to implementation, facilitation and assessment. There are also tutorials that serve as background information for various PCOL modules. There are occasional problems with broken links on this site. For example, athough the index is supposedly searchable by the first letter of the topic, clicking on the letter brings the user to a dead end (broken links page at Monmouth University). Overall, this is a valuable resource for those faculty members interested in providing a guided inquiry and collaborative experience for physical chemistry students. Rating: 5.0/5 (1 vote cast) |
Method OIA-1677 Available Cyanide by FIA, Ligand Exchange and Amperometry
by EPA Details This is a pdf version of an official EPA method for the analysis of cyanide. It discusses a variety of quality control procedures a wide range of controls that must be used for method maintenance and development. Within the context of teaching, this site could be viewed as unique in allowing students to work through all contingencies that must be moniitored for a measurement to be deemed valid. It defines and contains a variety of control parameters with mathematical descriptors. The chemistry for the flow injection analysis of cyanide is provided as well as a diagram of the instrumental setup. Cyanide is widely dispersed in the environment and its analysis should be of interest to students. Rating: 2.0/5 (2 votes cast) |
Applications Searchable Site
by Waters Corporation Details This site is a search engine for chromatographic and mass spectral methods in the Waters Corporation database. It searches based on analyte. It pulls up refereed journals(citations only) and company literature (pdf format). The site claims 23,500 documents. The site will be useful to those looking for methods in chromatography, including faculty and students looking for project ideas for either research or laboratory experiments. Rating: 1.0/5 (1 vote cast) |
Synthesis of a Sonogel-Carbon Modified Sensor Electrode with Titanium Oxide (TiO2) to Detect Catechol
by Suzanne Lunsford Details This experiment demonstrates cyclic voltammetry, surface modification, selectivity, and bioanalysis in assaying catechols in the presence of ascorbic acid. Pre- or post-lab questions are included, along with sample student data and instructor's notes. Rating: 1.0/5 (1 vote cast) |
Instrumental Analysis Experiments
by Walters, John P. Details Laboratory experiments for undergraduate instrumental analysis. Topics include data acquisition, control of instrumentation (gas chromatography, polarography, voltammetry, atomic absorption, robots), infrared spectroscopy, liquid chromatography, and nuclear magnetic resonance. Extensive use of LabView, Excel, and computers. Experiments are in PDF format. Rating: 1.0/5 (1 vote cast) |
Gas Chromatography experiment
by Wayne E. Steinmetz Details This site provides a Word document that describes a GC experiment involving the separation and quantitation of four butyl alcohol isomers. It has a complete background about the components of a GC instrument (with labeled pictures) and their functions. It has a section devoted to the measurement of response factors of the detector in use (here an FID). This would be a good experiment for a new faculty member to use as is, with slight modification to make it relevant to the particular GC system to be used. Rating: 4.0/5 (1 vote cast) |
Paper Chromatography of Stains
by Virzi, Frank Details A paper chromatography experiment separating dyes. The experiment is targeted toward 8-12 grades, but could be suited to an introductory chem laboratory section.The text of the site contains instructions for setting up and executing the experiment in a large class setting. Rating: 1.0/5 (1 vote cast) |
Infrared Spectroscopy
by Wooster Polytechnic Institute Details Provides an introduction to the theory of molecular vibrations and discusses applications of infrared spectral measurements at the level of a freshman or sophomore text book. Rating: 1.0/5 (1 vote cast) |
NMR Spectroscopy: Lab 8
by Sergei N. Smirnov Details A complete NMR laboratory exercise from a set of fifteen (15) experiments in various topic areas developed for a physical chemistry laboratory at New Mexico State University. Excellent introductory material is provided, along with links to additional sources of information, including NMR tutorials. Pre-lab questions are presented along with detailed laboratory procedures. The two part experiment has students first measure proton spectra for a set of unknown substances and to match the spectra with the compound in a list provided, followed by a kinetics measurement. While the procedure is specific to Varian instruments, users should be able to easily modify the parameters to their own instrument. Site authorization is required to use some of the embedded links, but even without that access, this experiment should be of interest to instructors in both instrumental or physical chemistry. Rating: 3.0/5 (1 vote cast) |
Learning to Learn: An Introduction to Capillary Electrophoresis
by Mabrouk, Pam Details This article describes a problem based learning approach to analytical chemistry labs using capillary electrophoresis as the instrumental method. The on-line link requires a password for The Chemical Educator to get the full article. The article also describes a lab that is an example of problem based learning. Students, playing the role of lab technicians, learn how to use the instrument in order to perform an analysis. Rating: 1.0/5 (1 vote cast) |
Micro Separations Distance CE
by L. A. Holland, C. M. White, K. M. Hansen Details This site describes how to assemble an inexpensive, yet reliable capillary electrophoresis apparatus and provides experiments to demonstrate electrodynamically-driven separations. Good background material about CE theory is provided. Rating: 4.0/5 (1 vote cast) |
Quantitative Chemical Analysis, 6e
by Harris, Daniel C. Details This is a site with material related to Dan Harris' textbook. It is not as general as some sites but the material is of high pedagogical value. Short tutorial sections are available for many topics with extensive web linkages. "Living" graphs and Excel files illustrate important material such as pH fractional composition and statistical analysis. Students can take practice quizzes on material from the text. Full Powerpoint slideshows include nearly all of the figures contained in the text. Full set of laboratory experiments are available. Some material is not available without registering as a user. Some menus are hidden beneath buttoms of windows, and are sometime difficult to utilize. Once mastered, the site works well. The most likely users of this site are teachers and students who may be using Harris' textbook, as much of the material is keyed to it, but others may also find it useful. Rating: 4.0/5 (1 vote cast) |
Chrom. and Electrophoresis experiments with PDFs
by CENTER for CHEMISTRY EDUCATION Details A site with PDF links to several slab gel electrophoresis, HPLC, and GC experiments intended for high school or college audiences. This site may provide a useful starting point for faculty seeking to implement new laboratory experiments based on these techniques. A login (email address) is required, but once logged in, follow the "Free Resources" link to see many instrumental and analytical experiments that have been submitted to the site. Rating: 3.0/5 (1 vote cast) |
CASE TEACHING NOTES for Filthy Lucre
by Ed Acheson Details The website presents a case study involving the detection of cocaine on dollar bills. The case study uses GC-MS, but has an introduction appropriate for beginning chemistry students. Rating: 2.0/5 (1 vote cast) |
An Unusual Arson Case: Polymer Grains
by Gino Van Vaerenbergh Details A case example of determination of an arson accelerant by a variety of analytical techniques. Will make a good case record for an active learning class. Uses a variety of techniques, particularly chromatography and headspace analysis. Rating: 3.0/5 (1 vote cast) |
Chemistry 160: Physical Measurements and Analysis
by Wayne Steinmetz Details Site contains lab experiments for both analytical and physical chemical measurements. There are 6 analytical experiments: data acquisition, AAS, voltammetry, ASV, GC-MS, stop-flow kinetics and HPLC. Experiments use real samples and are ready for implementation. Rating: 3.0/5 (1 vote cast) |
Affinity Chromatography
by DiResta, Dan Details This is an experiment showing the application of affinity chromatography to the separation of albumin from horse serum. A brief introduction of affinity chromatography and how it is being used in this specific experiment is given. This appears to be a good experiment to show the advantages of affinity chromatography in separating specific proteins from a complex matrix and would be useful in a biochemistry course or a course that is specifically looking at differing types of chromatography. Rating: 4.0/5 (1 vote cast) |
analytical chemistry lab manual
by David Henderson Trinity College Details This is a lab manual for an undergraduate analytical laboratory course. Experiments include fairly typical exercises such as acid/base titration, EDTA titrations, liquid chromatography analysis of chocolate (caffeine, theobromine, vanillin), vanillin by spectrophotometry (solvent extraction + solid phase extraction), ion selective electrodes, and GC of fatty acids via derivitization. Note that some of the supplementary materials referred to in the manual are posted in Blackboard and are unavailable to the public. Rating: 4.0/5 (1 vote cast) |
GEM: Greener Education Materials for Chemists
by Julie Haack Details This site is a resource for green chemistry principles and literature. It provides links for making green organic experiments and teaching the principles of green synthesis. Although it does not have many links specifically to chemical analysis, it provides an extensive overview and source of information regarding the important area of green chemistry. Rating: 3.0/5 (1 vote cast) |
Electrochemistry and Detection of Organic and Biological Molecules such as Catechols
by Suzanne Lunsford Details This ASDL online article describes a lab experiment whereby students learn how to prepare a conducting thin-film polymer electrode for the analysis of catechol and the effect of ascorbic acid on the cyclic voltammetric results. Rating: 4.0/5 (1 vote cast) |
Flow Injection Analysis in the Undergraduate Laboratory
by F. R. P. Rocha and Joachim A. Norbriega Details This paper titled, Flow Injection Analysis in the Undergraduate Laboratory, by Rocha and Nobrega was published in the Chemical Educator. It describes two basic experiments. One is the measurement of copper using PAR reagent as carrier in a single line FIA system. Increasing the reaction coil length results in double peaks. Refractive index effects are demonstrated in the two-line system by adding ethanol. The second experiment is the measurement of phosphate with the molybdenum blue reaction in a three-line system. The effect of temperture is demonstrated, showing also the formation of bubbles at higher temperatures. The experiments are designed for a 4-hour laboratory. Unfortunately, the supplmentary PDF, which contains the schematic for the sliding-bar injector, is only available for Chem. Educator subscribers (or possibly by contacting the authors). This is a useful lab experiment for undergraduate quantitative analysis or instrumental course. Rating: 3.0/5 (1 vote cast) |
Educator's Reference Guide for Electrochemistry
by Pine Instrument Co. Details This is a 70 page primer on analytical electrochemistry of interest to faculty, students and practitioners wanting to learn about basic concepts and applications. Rating: 4.0/5 (2 votes cast) |
SPECTROPHOTOMETRIC DETERMINATION OF ASCORBIC ACID IN ...
by M. Umar Dahot et al. Details An article that describes the flow injection analysis determination of ascobic acid using iron phenanthroline as a redox reagent and UV vis detection. Rating: 4.0/5 (1 vote cast) |
Spectroscopy
Details This site describes the theory and practice of IR and NMR spectroscopy for classroom and laboratory instruction. Although it is written for a course at the University of Colorado, Boulder, this site is appropriate for anyone doing analytical measurements with infrared or NMR. Rating: 3.0/5 (1 vote cast) |
Forensic Science Laboratory
by Rob Thompson Details This site has been accepted as the first on-line labbook in ASDLib. It presents analytical instrumentation in a forensic context, so that students learn both about quality measurements and the logic of combining results to draw conclusions. Rating: 4.0/5 (2 votes cast) |
Coal Sampling
by D. W. Golightly and F. O. Simon Details This USGS method explains the use of fluxes for preparation of coal for elemental analysis. Useful to supplement textbooks concerning sample preparation and may be useful in designing an XRF laboratory experiment. Rating: 3.0/5 (1 vote cast) |
Integration of Environmental Analytical Chemistry with Environmental Law: The Development of a Problem-Based Laboratory
by Devon A. Cancilla Details This JCE paper is well written, generous referenced and will serve as an excellent reference for anyone interested in adapting and implementing this problem-based approach to an upper-level environmental analysis laboratory that emphasis QC/QA and performance-based analytical methods. Rating: 3.0/5 (1 vote cast) |
Cyclic Voltammetry
by Kennesaw State University Details This site provides an excellent experiment involving cyclic voltammetry at a gold electrode. The experiment includes a detailed introduction to the topics of electrode capacitance, electrode reactions, and flux of the electroactive species to electrode surface. Lab report guidelines and post-lab questions are included. Rating: 3.0/5 (1 vote cast) |
Experiments in Electrochemistry
by Giorgio Cargoni Details Experiments with batteries, made from readily available materials, are designed for upper elementary and high school students to learn about the rudimentary principals of electrochemistry. Rating: 4.0/5 (1 vote cast) |
The Fluoride Ion Selective Electrode Experiment
by David L. Zellmer Details This is an experiment for the determination of fluoride ion with an ion selective electrode (ISE). While some experimental guidelines are given, students are left to choose appropriate standard concentrations and sample type, and to develop their own experimental procedure. Rating: 1.0/5 (1 vote cast) |
Determination of DNA Bases Chemistry: A Discovery-Based Experiment
by Richter, Mark M. Details The paper contains details of an electrochemistry lab where students are given the time to explore and design an experiment to identify the different DNA bases. The paper has a very useful compendium of literature relating to electrochemical techniques. Rating: 1.0/5 (1 vote cast) |
Cyclic Voltammetry
by Severin, Kathryn G. Details This site provides an excellent experiment involving cyclic voltammetry at a gold electrode. The experiment includes a detailed introduction to the topics of electrode capacitance, electrode reactions, and flux of the electroactive species to electrode surface. Lab report guidelines and post-lab questions are included. Rating: 1.0/5 (1 vote cast) |
Introduction to Lasers
by Carol Korzeniewski Details Lasers are preferred light sources for high resolution or time-resolved optical spectroscopy. This module introduces the workings of lasers and gives examples of common designs. Rating: 0.0/5 (0 votes cast) |
Introduction to Signals and Noise: eLearning Module
by Steve Petrovic Details Basic concepts of signals, noise, and extraction of data from noisy signals are presented as an e-learning module. Excel spreadsheets allow students to vary noise parameters. Basic electronics ideas relating to RC circuits support introductory information on filters Rating: 0.0/5 (0 votes cast) |
Multiple Regression
by Alan Fielding Details This site provides an introduction to the use of multiple regression, beginning with a glossary of important terms before taking the reader through a review of bivariate regression and the implementation and interpretation of multiple regression. One limitation to the site is its reliance on Minitab for calculations. Users, however, can reproduce the calculations using other software packages, such as SPSS or Excel. Prior knowledge of the basics of bivariate regression is assumed; thus, the site is most appropriate for advanced undergraduates and graduate students. Rating: 3.0/5 (1 vote cast) |
Principal Component Analysis
by Alan Fielding Details This site provides an introduction to principal component analysis, beginning with a glossary of important terms before taking the reader through the process of completing a principal component analysis. One limitation to the site is its reliance on Minitab and SPSS for calculations. Users without access to these programs can reproduce the calculations using other software packages, such as the freeware program R. Prior knowledge of basic statistics is assumed; thus, the site is most appropriate for advanced undergraduates and graduate students. Rating: 4.0/5 (1 vote cast) |
ELISA Animated Virtual Laboratory
by Howard Hughes Medical Institute Details This animated virtual laboratory, produced by HHMI, addresses concepts related to analytical immunoassay including the basis of humoral immunity,the foundation of ELISA, potential errors in conducting an ELISA and the sensitivity and specificity of diagnostic tests. This site has several layers including a laboratory notebook that provide experimental protocols for each step. This animation requires Shockwave to view, which is available as a free download. Rating: 4.0/5 (1 vote cast) |
Optics Tutorial
by Jeremy Learner and A. Thevenon Details This site provides a tutorial on electromagnetic waves using animated graphics. The tutorial gives the student the ability to visualize circularly polarized waves, the superposition of various types of polarized waves, and the change that results when the EM waves interact with matter. Rating: 0.0/5 (0 votes cast) |
Quality in Environmental Analysis
by U.S. Geological Survey Details Although this website by the U.S. Geological Survey (USGS) does not contain analytical data or methods per se, it is one that contains a complete compendium of links to material on environmental topics under the pervue of USGS. As such, it can serve as a resource and background material for students, faculty or practitioners interested in learning about environmental issues. For example, there is a link to Hg in the environment that discusses the sources, chemical composition and consequence of Hg as related to land or water species. This site is a library of links to USGS articles and reports, some of which may not open. Otherwise, it is easy to browse and link to topics of interest. Rating: 0.0/5 (0 votes cast) |
Introduction to Data Analysis
by David Harvey Details Means, standard deviation, and deciding if two results are different at some level of statistical significance is the basis for analytical decision making. This module teaches students how to use t-tests, Q-tests, and to tell when differences are statistically real. Rating: 5.0/5 (1 vote cast) |
Fundamentals of GC/MS
by Shimadzu Europa GmbH Details This tutorial provides an excellent introduction into the fundamentals of GC/MS. The tutorial consists of five sections: An introduction of mass and types of ions, ionization modes, hardware, figures of merit describing mass analyzer performance, and qualitative methods of GC/MS analysis - including library searches. Each section contains animations or simulations of chemical and physical interactions that pertain to mass spectrometry such as gas-phase ionization processes, fragmentation, mass analyzers, the importance of a vacuum, and detectors. A basic introduction to gas-liquid chromatography is also provided. The tutorial is intended to describe GC/MS at an introductory level, but does include theory at an intermediate level, which may be included or not depending on the intended audience. Information is presented in a Powerpoint style, and each figure has a Details tab which provides additional information on the subject. This website has excellent pedagogical value for students and new practitioners. Rating: 3.0/5 (1 vote cast) |
X-ray Diffraction
by Peter Goodhew Details This site is a good freshman or sophomore level introduction to diffraction and its application to studying crystal structure. Because it's very visual and interactive, it engages the student. It's not mathematical enough for an upper level course. The basics of diffraction are covered with excellent interactive demos. Demos are great as a supplement but not as a stand alone module on diffraction. Rating: 0.0/5 (0 votes cast) |
Simplex Optimization Methods
by Grabitech Details This site, from the developers of the software program Multisimplex, provides a basic introduction to simplex optimization. Topics include the basic simplex method, the modified simplex method and evolutionary optimization. Although the mathematical details are not included, the site provides flow charts showing the logic behind the optimization. The site assumes that the user understands the need for optimization and, therefore, is less suitable for beginners. Rating: 0.0/5 (0 votes cast) |
Micro- and Nano Technology, 1st Int'l Symp 2004
by Tuan Vo-Dinh Details Technologies developed at Oak Ridge National Laboratory include: 1) use of nanoprobes based on plasmon-resonance (which is defined) to enhance surface Raman scattering and fluorescence; 2) an optical neurosensor based on a 40 nm fiber optical tip; and 3) a multifunctional biochip capable of DNA and other protein-based bioassays. The article is written in PDF format with several illustrative graphics. Although insufficient in details to duplicate experimentally, the article does provide a nice overview of how development of small-scale analytical measurements can be used to address important biological problems. This 6 page article is a paper that was presented at the 1st Int'l Symposium on Micro and Nano Technology in 2004. A list of references appears at the end. Rating: 0.0/5 (0 votes cast) |
Introduction to AFM
by David Carberry Details Excellent introduction to the technique of atomic force microscopy at a level suitable for undergraduates. The page describes the basic modes (constant force, tapping, lift mode) and explains the significance of the tip and tip effects in imaging. Rating: 0.0/5 (0 votes cast) |
HPLC, LC-MS, and FTIR sites
by Shula Levin Details This site contains a considerable amount of information on HPLC, LC-MS, and FTIR via linked sites by the same author and some vendor sites. It may require considerbale time to follow the links to find specific information, but as a collection of sites related to HPLC and FTIR it is quite useful as a teaching resource. There are some interesting animations that might be helpful for students to understand how these instruments work. Rating: 0.0/5 (0 votes cast) |
Exclusion Chromatography
by Kimball, John W. Details This site contains a brief description of the separation mechanism in size exclusion chromatography. The picture helps visualize the separation, but is a simplified and idealized presentation. A companion site, http://users.rcn.com/jkimball.ma.ultranet/BiologyPages/A/AffinityChrom.html, describes affinity chromatography. The two sites together may be helpful in a biochemistry course where such techniques are used or discussed. Rating: 0.0/5 (0 votes cast) |
Reverse Phase HPLC Basics for LC/MS
by Ion Source, LLC Details This site provides a tutorial on practical reverse phase chromatography for LC-MS. Focusing on peptide and protein analysis, Andrew Guzzetta offers appropriate tips on mobile phase gradients, preparing your reversed-phase HPLC column for the first run of the day, and taking care of your column after the day's separations are complete. The site also provides a representative list of web-based resources on LC. Rating: 0.0/5 (0 votes cast) |
Experimental and Teaching Modules
by EAMNET Details The site contains a set of experimental and teaching modules that cover the fundamentals, history and practice of microscopy. Modules on microscopy, FRET, FRAP and Quantitative Multidimensional Microscopy will be of interest to chemists and biologists. Several include great graphics that would be helpful additions for instrumental analysis lectures. Rating: 0.0/5 (0 votes cast) |
Statistics for Chemists
by R. Wehrens Details Excellent comprehensive resource on statistics, including information on descriptive statistics, confidence intervals, hypothesis testing, regression, ANOVA, experimental design, and multivariate statistics. Web-based exercises are interspersed throughout the text, allowing students to practice what they are learning and to obtain immediate feedback. Rating: 0.0/5 (0 votes cast) |
Statistics for Analytical Chemistry
by Scott van Bramer Details This site provides a brief reference on statistics that both analytical faculty and students will find useful. The site includes a series of problem sets and supporting MathCAD spreadsheets. Materials available on the website can be downloaded as a pdf file. Rating: 0.0/5 (0 votes cast) |
ICP Operations: A Guide for New ICP Users
by Dr. Paul Gaines Details A handbook for ICP analysis. Topics such as matrix compatibility, quality control, spectral interferences, instrument operation (e.g. sample introduction, nebulization, etc.) make this an excellent practical yet concise manual on ICP operation. Rating: 0.0/5 (0 votes cast) |
Flow Injection Analysis
by Monash University Details This website by Monash University provides a primer for those who are beginners as well as those who wish to have a refresher on the principles and illustrative applications of flow injection analysis (FIA). The left hand menu allows selection of topics: FIA, Princples, Dispersion Process, Modes of Applications, Recent Developments, Bibliography and People in FIA. Schematics and illustrative signal outputs are provided for each FIa method. The site is easy to browse with links to subtopics. The site is unique in terms of bringing together in one place the basics of FIA with illustrations. Rating: 0.0/5 (0 votes cast) |
SPR : Surface Plasmon Resonance Tutorial
by Arnoud Marquart Details Provides a straightforward introduction to the fundamentals of SPR, the genesis of the plasmon and the evanescent wave, and how SPR can be used to monitor the chemical nature of species adsorbed to the surface of a metal substrate. Rating: 0.0/5 (0 votes cast) |
GlobalFIA
by GlobalFIA Details This site by GlobalFia provides a tutorial on the general aspects of flow injection analysis (FIA), sequential injection analysis (SIA) and the newly coined zone fluidics. Thus, it serves as an excellent resource for teaching flow methods to both undergraduates and graduate students, and as a refresher to practitioners. The tutorials are divided into 9 sections: introduction, fundamentals, dispersion, enrichment, chemistry, SIA, zone fluidics and bibliography. This modular approach makes information on concepts easy to digest and builds sequentially on each previous module with accompanying illustrative graphics. The bibliography provides references to hardcopy primary sources and a link to the FIA database at U. North Florida. The step-by-step instruction for the development of a new SIA method could be very helpful to someone who may be starting a new system or wishing to develop and new experiment. The site is easy to browse. Rating: 0.0/5 (0 votes cast) |
Principal Components Analysis Tutorial
by Lindsay I. Smith, Dept CS, U of Otago Details This site provides a clear introduction to the principle component analysis (PCA) without overwhelming the student. The tutorial includes a brief introduction and an explanation of the mathematics of PCA. Rating: 0.0/5 (0 votes cast) |
Spectroscopy
Details This site describes the theory and practice of IR and NMR spectroscopy for classroom and laboratory instruction. Although it is written for a course at the University of Colorado, Boulder, this site is appropriate for anyone doing analytical measurements with infrared or NMR. Rating: 3.0/5 (1 vote cast) |
Potentiostats
by Bank Electronik Details This PDF document (52 pages) provides a comprehensive discussion of background history, theoretical considerations, electronic circuitry and design of potentiostats. Subject is treated in depth not found in textbooks, although computerized formats are not included. Rating: 0.0/5 (0 votes cast) |
Analyzing Ligand-Protein Binding
by Dr. Harvey Motulsky, President, GraphPad Software Details This website consists of a text file that describes the analysis of radioligand binding experiments in a step-wise, easy to follow sequence. Although this site will be most useful to students trying to understand radioligand binding, the discussion is applicable to other types of ligand-protein binding experiments. The site also discusses the limitations of Scatchard plots for data analysis and the importance of nonlinear fitting of binding data. Rating: 0.0/5 (0 votes cast) |
Flame Atomic Absorption
by G. Ma and G. W. Gonzalez Details In addition to being an introductory tutorial on Atomic Absorption Spectroscopy, the parent site has links to a variety of materials on environmental analysis including immunoassay, ICP, ISEs, mass spectrometry, ground water monitoring, soil sampling and so on. The index link for the parent site seems to be broken, but the other topics can be accessed using the next topic button on the bottom of each page. Rating: 0.0/5 (0 votes cast) |
Chemical Equilibrium in the Gas Phase
by Gwen Sibert, Roanoke Valley Governor's School Details This website describes gas phase equilibrium chemistry and provides a tutorial on key concepts like LeChatelier's principal and includes on-line exercises in which the reader can check their understanding. Calculations of equilibrium constants expressed in terms of pressure and concentration are presented. This site will be most useful for high school and introductory university Chemistry courses in which students are developing an understanding of equilibrium chemistry. Rating: 0.0/5 (0 votes cast) |
Surface Science Tutorials
by Simon Morton, Lawrence Berkeley Laboratory Details The Surface Analysis Forum contains tutorials, databases containing reference values important for many surface analyses, and a glossary for surface science technique acronyms. The tutorials are really on-line courses offered in specific aspects of surface analysis. All are presented in a clear fashion. In addition, there is a link to software (much of it free and downloadable) for data analysisThe site is structured for teaching and is easy to read. Rating: 0.0/5 (0 votes cast) |
Integration of Environmental Analytical Chemistry with Environmental Law: The Development of a Problem-Based Laboratory
by Devon A. Cancilla Details This JCE paper is well written, generous referenced and will serve as an excellent reference for anyone interested in adapting and implementing this problem-based approach to an upper-level environmental analysis laboratory that emphasis QC/QA and performance-based analytical methods. Rating: 3.0/5 (1 vote cast) |
Electromagnetic waves and circular dichroism:an animated tutorial
by Szilagyi, Andras Details This website provides a tutorial on electromagnetic waves using animated graphics. The tutorial gives the student the ability to visualize, plane, and circularly polarized waves, the superposition of various types of polarized waves, and the change that results when the EM waves interact with matter. Rating: 0.0/5 (0 votes cast) |
IR Helper
by Colby Chemistry Department Details JCAMP formatted spectra and javascript are used to lead the user through the analysis of IR spectra. The software asks the user a series of questions about the spectrum, and provides correction if the user answers incorrectly. Rating: 0.0/5 (0 votes cast) |
Statistics for Chemists: Exercises
by Wehrens, Ron Details This website contains a group of exercises that allow students to practice basic statistical calculations for descriptive statistics, confidence intervals, hypothesis tests, regression and experimental design. The exercises are interactive and provide feedback for students who submit wrong answers. Rating: 0.0/5 (0 votes cast) |
Improving the Art and Practice of Amino Acid Analysis
by Crabb, John W. Details This site presents a very detailed tutorial on amino acid analysis. Topics discussed include analytical methods, calibration, hydrolysis, sample preparation, reduction of background and contamination, calculations and references. This site will be especially useful for faculty and students at all levels interested in bioanalysis and especially in the practical aspects of amino acid analysis. Rating: 0.0/5 (0 votes cast) |
Tunable Monochromator Movie
by Thomas G. ChasteenChasteen Details This Quick Time movie illustrates and describes to operation of a Czerny-Turner monochromator. The slits, mirrors, grating and grating scan are described in the production of a specific wavelength at the outlet slit. The movie is a companion to the double beam spectrometer animation. Rating: 1.7/5 (3 votes cast) |
Affinity Chromatography
by Sapna Deo Details Using exposition, graphics, and commercial videos, this module teaches the theory and application of affinity chromatography in the characterization of proteins, nucleic acids, and other biochemical/biomedical systems. Problems and application examples support the tutorial material. Rating: 0.0/5 (0 votes cast) |
RSC.org: UV/Vis Spectroscopy
by The Royal Society of Chemistry- Univ. Warwick Details This video distributed on YouTube is on the basic principles of UV/Vis. Provides a good primer (~5 min), and the “top-off” look of the instrument is useful in explaining components. A double beam instrument is described. Rating: 4.0/5 (1 vote cast) |
RSC.org: Gas Chromatography
by The Royal Society of Chemistry- Univ.Warwick Details This video, distributed on YouTube by the Royal Society of Chemistry is on the basic principles of GC. This video is a short primer (~5 min) which introduces the technique and instrumentation.
There are many assumptions that are made in the presentation of this material, due to the fact the video is meant to be a basic introduction. Examples of such assumptions include the statement that volatility solely controls the elution order of volatile compounds on a GC column and that concentration is the only parameter that controls the relative response of a compound for a given GC detector. The ultimate strength of this video is the general nature of the content that makes it appealing to a wide audience. The video may be most appropriate in a lower-level general education science course (i.e forensic science) or as a quick orientation video for instrumental analysis students. The GC-FID and GC-MS are highlighted. Rating: 3.0/5 (1 vote cast) |
RSC.org: Proton NMR
by The Royal Society of Chemistry - Univ. of Warwick Details This video, distributed on YouTube by the Royal Society of Chemistry is on the basic principles of NMR. This video is a good primer and would be very useful to supplement introductory lectures on NMR. The video covers the basic theory behind a 1H spectrum and goes through actually acquiring a spectrum. The “top-off” look of the instrument is useful and how the superconducting magnet is mounted. Good for a basic introduction. Rating: 4.0/5 (1 vote cast) |
RSC.org: IR Spectroscopy
by The Royal Society of Chemistry-Univ. Warwick Details This video on YouTube covers the basic principles of infrared spectroscopy. Very useful for a newcomer to IR. This video of 6.5 minute would be useful in a classroom setting or students interested in the technique. Rating: 0.0/5 (0 votes cast) |
RSC.org: Mass Spectrometry
by Royal Society of Chemistry- Univ. Warwick Details This video, distributed on YouTube by the Royal Society of Chemistry is on the basic principles of mass spectrometry, using a magnetic sector instrument to demonstrate how specific m/z ratios can be selected. The theory and operation of MS, including the chemistry of ionization and fragmentation is described at an introductory level. There's also an excellent example of the use of high resolution MS to differentiate between nominal mass and actual mass. The video does a very good job of explaining the concept such that only a little background knowledge is required. The video is short enough (6 mins), that it would be very useful in a class setting or for students outside of class. The ultimate strength of this video is the general nature of the content that makes it appealing to a wide audience. The video may be most appropriate in a lower-level general education science course (i.e forensic science) or as a quick orientation video for instrumental analysis students prior to introducing mathematical or operational concepts. This video would also be helpful for a lay science person who wishes to learn more about mass spectrometry from a general interest perspective. Rating: 0.0/5 (0 votes cast) |
HPLC
by royal society of chemistry-University of Warwick Details This video, distributed on YouTube by the Royal Society of Chemistry is on the basic principles of HPLC. This video is a short primer (~5 min) which introduces the basic technique and instrumentation. The theory of HPLC is described at a very basic level. Separation theory is presented in a qualitiative fashion, and both the mechanics and applications of HPLC were generally described. The ultimate strength of this video is the general nature of the content that makes it appealing to a wide audience. The video may be most appropriate in a lower-level general education science course (i.e forensic science) or as a quick orientation video for instrumental analysis students. Rating: 0.0/5 (0 votes cast) |
Atomic Force Microscopy
by Prof. Arvind Raman Details A video lecture on Atomic Force Microscopy (AFM) by Prof. Arvind Raman of Purdue University that discusses the historical development, instrumentation and operational principles of various AFM modes. The lecture is accompanied by power point slides with clear illustrative graphics. Basics are provided in the application examples with advantages and limitation discussed. Useful site to those interested in learning AFM. Rating: 3.0/5 (1 vote cast) |
Accelerator Mass Spectrometry in Biology and Health Care
by Lawrence Livermore Lab Details This video, developed at Lawrence Livermore National Laboratory, describes the instrumentation for accelerator mass spectrometry and its applications. The video describes the instrumentation and its application for carbon dating and measurements of drug distribution. Rating: 0.0/5 (0 votes cast) |
Gas Chromatography Video
by Frank Dunnivant, Whitman College, Education Solns Details This is a high quality video module demonstrating the basics of gas chromatography. Highlights include different GC instruments, detectors etc., as well as unique topics such as trouble shooting and interfacing the column that are not addressed in standard texts. This resource can be run (Shockwave Flash) from the home server or downloaded to your computer. Rating: 0.0/5 (0 votes cast) |
HPLC Tutorial 2,0 Video
by Frank Dunnivant, Whitman College, Education Solns Details This high quality video resource focuses on partition chromatography. The video presents an overview of basic separation theory and discusses instrumentation and data analysis. The size of the video (62.6 MB) almost requires a high speed internet connection. The resource can be downloaded to the user's computer, which is recommended for those with slower connections. Rating: 4.5/5 (2 votes cast) |
Virtual tour of a Forensic lab
by Court TV Details This virtual tour of a forensic laboratory has three floors. Each floor has a number of rooms devoted to a particular forensic specialty. Each room has a slide show of forensic scientists performing their work. All rooms have a video explanation detailing the forensic specialty being visited. Some rooms also have videos of forensic scientists demonstrating analytical techniques. Rating: 0.0/5 (0 votes cast) |
Videos zur Titration und Gravimetrie (Titration and Gravimetry Videos)
by TU Clausthal Details This website provides a set of short videos which demonstrate to quantitative analysis students the basic steps and visual changes encountered for the following experiments: Mohr titration (for chloride), acid-base titrations, and gravimetry for iron and nickel. A cursory knowledge of German is needed. However, individuals with some knowledge in these techniques can interpret these videos with little trouble. Real Player (or other software that can play .ram files) is required. Rating: 0.0/5 (0 votes cast) |
Quantitative NMR
by Cynthia Larive Details A learning module focused on principles and practice of NMR for quantitative analysis, an application less commonly associated with the technique than is structure determination. Links to simulation packages are included. Rating: 5.0/5 (2 votes cast) |
LabVIEW for Instrumental Analysis
by Mark Jensen Details This site provides two useful resources for instructors and students of analytical chemistry. The first is a collection of LabVIEW virtual instruments (VIs) for demonstrating topics such as signal-to-noise ratios, boxcar and ensemble averaging, power spectra, digital filtering, analog-to-digital conversions, and the Nyquest frequency. For users that do not have a working copy of LabVIEW, executable versions are included that use LabVIEW's free run-time engine (Windows only). The second set of resources is a series of tutorials for teaching students how to write their own VIs. The tutorials are well thought out and nicely build on each other. Rating: 0.0/5 (0 votes cast) |
ELISA Animated Virtual Laboratory
by Howard Hughes Medical Institute Details This animated virtual laboratory, produced by HHMI, addresses concepts related to analytical immunoassay including the basis of humoral immunity,the foundation of ELISA, potential errors in conducting an ELISA and the sensitivity and specificity of diagnostic tests. This site has several layers including a laboratory notebook that provide experimental protocols for each step. This animation requires Shockwave to view, which is available as a free download. Rating: 4.0/5 (1 vote cast) |
Ion Exchange Chromatography
by Paul A. Craig Details This website contains an ion chromatography simulator that can be run on-line or can be downloaded. The simulator focuses on separations of proteins using Ion Chromatography. Also included is hyperlinked reference information, an example of a homework assignment using the simulator, and some information on protein structures.(note this is an archived version of this site, as the original has been moved). Rating: 0.0/5 (0 votes cast) |
DNA Evidence Training
by National Commission on Future of DNA Evidence Details These training modules are intended to provide interactive training that covers basic information about the identification, preservation, and collection of DNA evidence at virtual crime scenes related homicide, sexual assault, and burglary. Information addressed in this interactive training program is delivered in two modules.
The Beginning Level Module focuses on issues that arise for the first-responding law enforcement officer.
The Advanced Level Module delivers more in-depth information for the evidence technician. Also included are test questions, a glossary, and references. Rating: 0.0/5 (0 votes cast) |
primer on microscopes
by Olympus Details This website is sponsored by Olympus company. It is similar to two other sites (one by Florida State University, the other by Nikon) already in asdlib whereby a common group of authors contributed to the development of all three sites. Thus, these sites are similar in content although differences exist. This Olympus site has a "virtual microscopy" that contains links to interacdtive tutorials that demonstrate the operation of different types of microscopes. Thus, one can compare how various types of microscopes work, play with controls, see how some settings can cause errors, etc. Optical microscopy per se is underutilized in the teaching of chemistry but is very important industrially. The site's applets and the way they are connected work well - a virtual lab that can be used effectively for instruction and learning. Rating: 0.0/5 (0 votes cast) |
Rice virtual lab in statistics
by David Lane Details This site is devoted to statistical tests and demonstrations of their use and was created with the support of the National Science Foundation. One section is a complete reference guide - the online statistics textbook, with detailed descriptions of all things statistical. The second, and most fun section, is simulations/demonstrations section where nearly twenty statistical tests are demonstrated with interactive Applets. Each Applet has clear instructions for use with details on the test demonstrated. A third section gives case studies where statistics have played a role, illustrating theory with specific analyses from court cases to who is buying iMacs. Rating: 0.0/5 (0 votes cast) |
SPR and Related Calculations
by Rob Corn Details Computation of Surface Plasmon Resonance using common surfaces (gold, silver, copper) and wavelengths (632.8 nm) is done on-line. The site is maintained for researchers and students alike. Rating: 0.0/5 (0 votes cast) |
Basic Concepts of Optical Microscopy
by M.W. Davidson and M. Abramowitz Details A comprehensive primer focused on the basic optical microscope, as well as the electron, confocal, polarizing, and stereoscopic microscopes. Virtual microscopes allow the user to simulate the use of a variety of real-life microscopes. There are galleries of photomicrographs illustrating a variety of specimens. This website provides complete instructional materials on the theory of light and the applications of microscopy to a variety of analytical problems. Rating: 0.0/5 (0 votes cast) |
VMSL: Virtual Mass Spectrometry Laboratory
by Joseph J. Grabowski Details This site presents a series of case studies that can be explored using modern mass spectrometry methods. The problem-solving nature of the site provides students a virtual laboratory experience that can supplement access to mass spectrometry instrumentation. Rating: 0.0/5 (0 votes cast) |
Chemistry Experiment Simulation, Tutorials and Computer Animations for College Chemistry
by Tom Greenebowe Details After instructions on what computer programs will be needed, you can simulate chemical processes related to electrochemistry, acid-base chemistry & stoichiometry. Rating: 0.0/5 (0 votes cast) |
PC Software for NMR, IR
by Bell, Harold M. Details This web site allows readers to download a variety of PC-based NMR simulation programs. NMRSM is for the calculation of spin-spin coupling patterns, the program FTNMR Simulator simulates the operation of a high field spectrometer and the program FIDMAKER allows the user to create FID's for subsequent analysis by students. Although these simulation programs are fairly limited in their scope, they will be useful for faculty at institutions that do not have access to a modern Fourier transform NMR spectrometer. Rating: 0.0/5 (0 votes cast) |
Introduction to Chemical Equilibria
by Blauch, David N. Details An interactive set of applet-based demonstrations (many modeled as experimental measurements) that illustrate the concepts and calculations of chemical equilibria. The site demonstrates equilibrium processes in a reaction vessel by plotting the concentration of reactants and products over time. The site would be a good supplement for a class in general chemistry or quantitative analysis. Rating: 0.0/5 (0 votes cast) |
Introduction to Lasers
by Carol Korzeniewski Details Lasers are preferred light sources for high resolution or time-resolved optical spectroscopy. This module introduces the workings of lasers and gives examples of common designs. Rating: 0.0/5 (0 votes cast) |
Photodetectors and Fiber Optics
by Ken Crozier Details Power point slides to support a lecture on the principles and usage of photodiodes and optical fibers for sensors and instrumentation. There is no supporting text for the slides. Rating: 0.0/5 (0 votes cast) |
Atomic Force Microscopy
by Prof. Arvind Raman Details A video lecture on Atomic Force Microscopy (AFM) by Prof. Arvind Raman of Purdue University that discusses the historical development, instrumentation and operational principles of various AFM modes. The lecture is accompanied by power point slides with clear illustrative graphics. Basics are provided in the application examples with advantages and limitation discussed. Useful site to those interested in learning AFM. Rating: 3.0/5 (1 vote cast) |
Anodic Stripping Voltammetry
by Michigan State University Details Site provides basics with illustrations of what happens during deposition and stripping of metals for analysis by anodic stripping voltammetry (ASV). The PDF presentation is easy to navigate and understand. It can be used as a supplement to a lecture or lab. Rating: 0.0/5 (0 votes cast) |
Virtual tour of a Forensic lab
by Court TV Details This virtual tour of a forensic laboratory has three floors. Each floor has a number of rooms devoted to a particular forensic specialty. Each room has a slide show of forensic scientists performing their work. All rooms have a video explanation detailing the forensic specialty being visited. Some rooms also have videos of forensic scientists demonstrating analytical techniques. Rating: 0.0/5 (0 votes cast) |
Green Chemistry (2nd edition)
by Stanley Manahan Details Measurement science used to characterize environmentally important species is a central aspect of this textbook and accompanying lecture support/PowerPoint presentations. In addition to discussing the hows and whys of measurement, the discussion of measurements up to 2007 as related to the future of the environment provides a context for learning the material. Rating: 0.0/5 (0 votes cast) |
Lead in DC Water
by Michael J. Clarke Details This site is a PowerPoint presentation describing the problem with lead in Washington, DC, drinking water. The presentation is interesting and well illustrated. It contains a discussion of the basic chemistry involved with this problem. It is potentially useful for a broad range of interests from high school through university level courses in environmental chemistry. It does not contain any significant amount of material on chemical analysis (lead determinations in water are well covered in other sources), but provides excellent rationale for the necessity of doing lead analyses in water. Rating: 0.0/5 (0 votes cast) |
Chemical Separations
by James K. Hardy Details This site contains complete notes in a PowerPoint-like presentation for a chemical separations course. It covers a wide variety of topics, including distillation, extraction, gas chromatography, liquid chromatograpy, chromatography theory, instrumentation, electrophoresis, field flow fractionation, and affinity chromatography. It covers these topics thoroughly using a clear, consistent, and simple presentation style. Links to major topics like GC, LC, and electrophoresis provide specific information about the theory, instrumentation, and practice related to these techniques. The site also contains many annimations illustrating important separation processes. Rating: 3.0/5 (1 vote cast) |
Chromatography Theory
by Thomas Hardy Details James Hardy has produced a number of powerpoint type lecture modules for analytical chemistry. This is another very good module that covers the introductory theory of chromatography. Includes chromatography types, plate and kinetic theories. Level of presentation is at the introductory analytical chemistry level. It is a colorful and well planned presentation of the introduction to chromatography that could be used as the basis for lectures on chromatography at the introductory analytical chemistry or instrumental analysis level. Rating: 0.0/5 (0 votes cast) |
Custom Designed HPLC Couse for Teva Abic
by Dr. Shulamit Levin Details This site contains slides to accompany lectures in HPLC. They do not contain enough description for the average student to follow. However, they provide a lot of excellent information about practical aspects of HPLC. The sections on troubleshooting, sample preparation, gradients, system peaks, system suitability and methods validation are particularily valuable. The illustrations and diagrams are informative but occasionally difficult to read because of their resolution. Applications and examples are very good. This site is a subset of Dr. Levin's larger site related to teaching separations and other analytical topics, but a link to her home page is provided. Rating: 0.0/5 (0 votes cast) |
Quantitative Chemical Analysis, 6e
by Harris, Daniel C. Details This is a site with material related to Dan Harris' textbook. It is not as general as some sites but the material is of high pedagogical value. Short tutorial sections are available for many topics with extensive web linkages. "Living" graphs and Excel files illustrate important material such as pH fractional composition and statistical analysis. Students can take practice quizzes on material from the text. Full Powerpoint slideshows include nearly all of the figures contained in the text. Full set of laboratory experiments are available. Some material is not available without registering as a user. Some menus are hidden beneath buttoms of windows, and are sometime difficult to utilize. Once mastered, the site works well. The most likely users of this site are teachers and students who may be using Harris' textbook, as much of the material is keyed to it, but others may also find it useful. Rating: 4.0/5 (1 vote cast) |
Chromatography
by Hardy, James K. Details This site provides fundamental background information about chromatogaphy, including plate theory, rate theory, the meachanisms of separations, and qualitative and quantitative aspects of chromatography. The format is a PowerPoint-like presentation. It is a subsite of a larger, broader site about chemical separations (http://ull.chemistry.uakron.edu/chemsep/index.html). The combination of all of the related sites is quite nice and students will find them useful. Rating: 0.0/5 (0 votes cast) |
Chromatography and Mass Spec Lectures
by Prof. Jose-Luis Jimenez , U. Colorado Details This site contains mass spectrometry and chromatography lecture notes for a graduate course. They are subdivided by topic (history, theory, etc.) and are easy to browse. They may be helpful to someone constructing their own course in chromatography and/or mass spectrometry. The notes are fairly complete. The historical sections may particularly save time in preparing courses. The notes also provide good information and a helpful outline to follow. The site also has some nice mass spectrometry animations from Thermo. Rating: 0.0/5 (0 votes cast) |
Fundamental measurement PowerPoint
by Mr. Allan Details This site contains good images of basic general chemistry lab equipment and how to use them to make measurements (graduated cylinders, burets, thermometers, and balances). It could be useful for introducing students to laboratory work and measurements. Rating: 0.0/5 (0 votes cast) |
Analytical Chemistry
by Henderson, David E. Details This site contains a list of detailed lecture notes covering a wide range of topics including equilibrium, titrations, sample preparation, acids and bases, buffers, spectrophotometry, potentiometry and chromatography. This site is part of a collection of notes from a general chemistry course taught at the State University of West Georgia. This well-linked page gives supplementary material that could be useful to intermediate chemistry majors in an analytical chemistry course or new faculty developing a course. Rating: 0.0/5 (0 votes cast) |
Experimental and Teaching Modules
by EAMNET Details The site contains a set of experimental and teaching modules that cover the fundamentals, history and practice of microscopy. Modules on microscopy, FRET, FRAP and Quantitative Multidimensional Microscopy will be of interest to chemists and biologists. Several include great graphics that would be helpful additions for instrumental analysis lectures. Rating: 0.0/5 (0 votes cast) |
EPR Basics and Application to Biology
by Thomas Prisner, University of Frankfurt Details This site contains a set of powerpoint slides that discusses the basic principles underlying electron paramagnetic resonance (EPR). The slides also present examples of the application of EPR to biological systems including organic radicals in proteins, paramagnetic metal centers and spin labels. Rating: 0.0/5 (0 votes cast) |
Learning Module: What Chemists need to know about copyright
by American Chemical Society Details This website, developed by ACS Joint Board/Council Committee on Copyrights, provides a learning module for chemists to learn about the legal aspects governing copyright and what constitutes copyright material. It contains a set of five useful resources: (1) an html learning module about copyright for chemists; (2) a set of questions faculty could use to test students' understanding of copyright; (3) a summary of copyright policy; (4) a pamphlet (pdf file) that could be handed out to a class for discussion; and (5) a copy of the ACS copyright transfer form (pdf file) that ACS publications use. Rating: 0.0/5 (0 votes cast) |
Atomic Absorption Instruction Module
by University of Michigan Dearborn Science Learning C Details An introduction to Atomic Absorption Spectroscopy for the non-chemist or new user. Rating: 5.0/5 (1 vote cast) |
Prediction of Chemical and Biological Properties of Organic Compounds from Molecular Structure
by Jurs, Peter C. Details This website is a PDF file of 32 slides and accompanying notes that describe the process of determining quantitative structure activity relationships. The slides focus on the ADAPT software, but are generally useful to anyone interested in QSAR, and discuss the details of Structure Entry and Molecular Modeling, Descriptor Generation, Feature Selection, Model construction, and Model Validation. Rating: 0.0/5 (0 votes cast) |
Molecular Structure and Dynamics by NMR Spectroscopy
by Edison, Arthur S. Details This site provides PowerPoint slides for a series of lectures for a graduate-level course in NMR spectroscopy. While the casual student may find it hard to follow everything on the slides without an accompanying lecture, the Power Point files should be very useful for advanced students or educators putting together similar courses. Mathematica documents that allow one to perform matrix algebra and Fourier transforms are also provided. Rating: 0.0/5 (0 votes cast) |
Chemometrics
by Hardy, James K. Details An overview of techniques used in data analysis. Basic statistics, analysis of variance, principal component analysis, neural networks, and multivariate calibration are addressed. Rating: 0.0/5 (0 votes cast) |
Radioanalytical Chemistry
by Hardy, James K. Details Course on the use of radionuclides in analytical chemistry. Types of radioactive decay are discussed as well as the techniques of scintillation counting, neutron activation analysis, and gamma spectroscopy. Rating: 0.0/5 (0 votes cast) |